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961.
Summary A method was developed for the determination of nitrobenzoic acids and nitrophenols as well as of diaminoaromatics and was
applied to the analysis of water samples from the former ammunition plant at Elsnig (Saxony, Germany).
The procedure is based on a preseparation into a neutral, an acidic and a basic fraction by multi-step extraction at different
pH values followed by HPLC analysis with UV and electrochemical detectors, coupled in series.
Applying optimized enrichment conditions, all investigated compounds were extracted from spiked distilled water with recoveries
>80% and variation coefficients <7%. Similar results were obtained with spiked ground water samples.
After enrichment, all compounds can be analysed by HPLC with UV detection at concentrations below 100 ngL−1. The electrochemical detector (ELCD) allowed a selective and sensitive detection of the nitrophenols and especially of the
diaminoaromatics and, therefore, provides, some advantages in the analysis of real samples.
Presented at the 21st ISC held in Stuttgart, Germany, 15th–20th September, 1996 相似文献
962.
用毛细管离子分析 (CIA)法 ,采用 10mmol·L- 1咪唑为背景电解质 ,4 0 %甲醇为选择性改性剂 ,在 pH 2 .5、分离电压为 2 5kV、柱温为 2 2℃的电泳条件下 ,采用间接紫外检测 (2 14nm ) ,在5min内测定了人发中铝 ,方法简便、快速、灵敏度高、重现性好、测定成本低 相似文献
963.
964.
Real-time visualisation of deformation fields using speckle interferometry and temporal phase unwrapping 总被引:1,自引:0,他引:1
A real-time system for analysing data from speckle interferometers, and speckle shearing interferometers, has been developed. Interferograms are continuously recorded by a digital camera at a rate of 60 frames s−1 with temporal phase shifting carried out at the same rate. The images are analysed using a pipeline image processor. With a standard 4-frame phase-shifting algorithm (phase steps of π/2), wrapped phase maps are calculated and displayed at 15 frames s−1. These are unwrapped using a temporal phase unwrapping algorithm to provide a real-time colour-coded display of the relevant displacement component. Each camera pixel (or cluster of pixels) behaves in effect as an independent displacement sensor. The reference speckle interferogram is updated automatically at regular user-defined intervals, allowing arbitrarily large deformations to be measured and errors due to speckle decorrelation to be minimised. The system has been applied to the problem of detecting sub-surface delamination cracks in carbon fibre composite panels. 相似文献
965.
R. Wilfinger J. Lettry A. Fabich H. Aiginger K. Poljanc R. Catherall M. Eller 《The European physical journal. Special topics》2007,150(1):373-378
Thermal stress-waves are generated in the solid target
material when the proton beam interacts. These stress waves excite
natural oscillations of the target or cause plastic deformations.
Hence, an experimental setup with a laser Doppler vibrometer
[CITE] was developed to investigate free surface
vibrations of cylindrical targets. The target configurations for
RIB and conventional neutrino beams (CNGS project) were
investigated to analyze proton induced thermal stress-wave
generation and propagation. 相似文献
966.
F. Pereira Dos Santos J. Léonard Junmin Wang C. J. Barrelet F. Perales E. Rasel C. S. Unnikrishnan M. Leduc C. Cohen-Tannoudji 《The European Physical Journal D - Atomic, Molecular, Optical and Plasma Physics》2002,19(1):103-109
We recently observed a Bose-Einstein condensate in a dilute gas of 4He in the 23S1 metastable state. In this article, we describe the successive experimental steps which led to the Bose-Einstein transition
at 4.7 μK: loading of a large number of atoms in a MOT, efficient transfer into a magnetic Ioffé-Pritchard trap, and optimization
of the evaporative cooling ramp. Quantitative measurements are also given for the rates of elastic and inelastic collisions,
both above and below the transition.
Received 15 October 2001 相似文献
967.
一种视频图像规则圆目标的超分辨率位置测量方法 总被引:4,自引:0,他引:4
介绍了一种用于视频图像规则圆目标的超分辨率位置测量方法。分析了超分辨率测量的原理 ,并提出和完成了测量方案 ,取得了满意的结果。首先在目标静止时 ,连续采集多帧视频图像 ,通过叠加平均进行降噪 ;其次通过罗伯特微分算子进行边界探测 ,求出目标的大致位置 ;最后通过边界重心拟合法、边界圆拟合法和最小二乘法拟合求出目标的精确位置。理论分析和实验表明 ,完整圆目标时 ,测量精度可达 1/4像素 ;而当目标图像有缺陷时 ,边界圆拟合法和最小二乘法拟合测量误差增加较少 ,边界重心法的测量误差增加较多。在具体情况下 ,算法及参数应该作相应的调整 相似文献
968.
HybridOptical-ElectronicImplementationofMorphologicalEdgeDetection¥YUANShifu;ZHANGXueru;ZHAOShijie;LIYan;CHENLixue(Department... 相似文献
969.
利用汞原子6~1S_0—7~1S_0双光子共振四波和频产生了125nm的相干辐射.对双光子共振增强效应、双光子共振克尔(Kerr)效应进行了研究.讨论了平面波和聚焦情况下最佳相位匹配的条件.实验中还观测到了四波参量振荡和四波差频的信号输出. 相似文献
970.
非线性RL电路的暂态特性 总被引:1,自引:0,他引:1
对一个可解的非线性RL电路模型的暂态过程进行了研究,得到非线性RL电路的一些普遍特性,加深了加RL电路中的有关概念的理解,对教学有一定的参考价值。 相似文献